Table of Contents
Title and "Recommended Text:
"Quantitative X-Ray Diffractometry" Lev S.Zevin, Giora Kimmel ed. Inez Mureinik
Springer-Verlag, New York, 1995".
Outline of Talk
Nomenclature - consistent with Klugg and Alexander
More Nomenclature
Introduction and Background
More background - absorption
Issues, types of analysis
Sample Features, Data Collection
Data Analysis
Basic Concepts
Basic Concepts, cont.
Techniques: relative, ratio
Techniques - 6 basic techniques to be described.
Technique#1: Absorption-Diffraction
Technique#1, cont.
Technique#1, cont.
Technique#1, cont.
Technique#1, cont., precision, detection limit.
Technique#2: Internal Standard Analysis
Technique#2, cont.
Technique#2, cont., precision, detection limit.
Technique#2, cont., Reference Intensity Ratio (RIR)
Technique#2, cont., Reference Intensity Ratio (RIR)
Technique#3: Doping or Spiking Method
Technique#3, cont.
Technique#3, cont.
Technique#3, cont.
Technique#3, cont.
Technique#4: Dilution Method
Technique#4, cont.
Technique#4: cont. precision and accuracy.
Technique#5: Complete n-phase analysis
Technique#5, cont.
Technique#5, cont.
Technique#5, cont.
"Also called external standard method (Hubbard C.R., Evans E.H, Smith, D.K., J.Appl.Cryst.,
9, 169-74, 1976)"
Technique#6: Whole Pattern Profile Matching
Technique#6: cont. Structure refinement
Technique#6: cont.
Notes of Interest: 1. Absorption and Microabsorption:
G. Cressey and M. Batchelder method.
Notes of Interest: 2. Quantitative Analysis with
Qualitative Control of Calibration Standards. T. Knudsen, X-Ray Spectrometry, 10 (2), 54-6, 1981.
Notes of Interest: 2. cont.
Notes of Interest: 2. cont.
Notes of Interest: 2. cont.
Bibliography
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Author: David Hay Email: hay@mst.csiro.au
MS Powerpoint to HTML: Lachlan Cranswick
CSIRO MST Home Page: http://www.mst.csiro.au/
CSIRO MST Materials Characterisation: http://www.mst.csiro.au/material/mc.htm
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